Tetrahydro-α-hydroxy-α-Methyl-2-(1-Methylethoxy)-5-oxo-2H-pyran-4-acetic acid Methyl Ester synthesis
- Product Name:Tetrahydro-α-hydroxy-α-Methyl-2-(1-Methylethoxy)-5-oxo-2H-pyran-4-acetic acid Methyl Ester
- CAS Number:1044244-99-6
- Molecular formula:C12H20O6
- Molecular Weight:260.28
600-22-6
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$6.00/5g
65712-89-2
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$1320.00/500mg
1044244-99-6
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$155.00/2.5mg
Yield:1044244-99-6 47%
Reaction Conditions:
with tributyl-amine;titanium tetrachloride in dichloromethane at -60 - -55; for 1.5 h;
References:
Nagase, Ryohei;Katayama, Mayumi;Mura, Hiroaki;Matsuo, Noritada;Tanabe, Yoo [Tetrahedron Letters,2008,vol. 49,# 29-30,p. 4509 - 4512]