3-AMino-5-[[(2,3-dihydroxypropyl)aMino]carbonyl]-2,4,6-triiodo-benzoic Acid synthesis
- Product Name:3-AMino-5-[[(2,3-dihydroxypropyl)aMino]carbonyl]-2,4,6-triiodo-benzoic Acid
- CAS Number:111453-32-8
- Molecular formula:C11H11I3N2O5
- Molecular Weight:631.93
122731-74-2
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111453-32-8
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$650.00/50mg
Yield:111453-32-8 90%
Reaction Conditions:
with sodium dichloroiodate at 75 - 85; for 5 h;
Steps:
2
Under stirring, the compound solution of formula VII and iodine monochloride sodium chloride solution (40%) 500g were added to the reaction bottle, and the control liquid was stirred at 75-85 °C for 5 hours. After the end of the reaction, the temperature was reduced to 15 ~ 20 °C stirred for 1 hour, filtered, dried to obtain 200g of compound VI, the yield was 90%.
References:
CN114195673,2022,A Location in patent:Paragraph 0083-0084; 0086
122731-58-2
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111453-32-8
37 suppliers
$650.00/50mg
1955-46-0
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$9.00/5g
111453-32-8
37 suppliers
$650.00/50mg