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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 5-(1-Butylbenz[cd]indol-2(1H)-ylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione
1151666-45-3

5-(1-Butylbenz[cd]indol-2(1H)-ylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione synthesis

3synthesis methods
2033-24-1 Synthesis
2,2-Dimethyl-1,3-dioxane-4,6-dione

2033-24-1
667 suppliers
$6.00/25g

5-(1-Butylbenz[cd]indol-2(1H)-ylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione

1151666-45-3
10 suppliers
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-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: triethylamine / ethanol
2: potassium carbonate / N,N-dimethyl-formamide / 18 h / 90 °C / Inert atmosphere

References:

Sinha, Sarmistha Halder;Owens, Eric A.;Feng, You;Yang, Yutao;Xie, Yan;Tu, Yaping;Henary, Maged;Zheng, Yujun George [European Journal of Medicinal Chemistry,2012,vol. 54,p. 647 - 659]

130-00-7 Synthesis
Benz[cd]indol-2(1H)-one

130-00-7
235 suppliers
$5.00/5g

5-(1-Butylbenz[cd]indol-2(1H)-ylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione

1151666-45-3
10 suppliers
inquiry

References
2-(methylthio)benzo[cd]indole

22546-91-4
5 suppliers
inquiry

5-(1-Butylbenz[cd]indol-2(1H)-ylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione

1151666-45-3
10 suppliers
inquiry

References