Benzoic acid, 4,4'-[(2,5-dimethoxy-1,4-phenylene)di-(1E)-2,1-ethenediyl]bis- synthesis
- Product Name:Benzoic acid, 4,4'-[(2,5-dimethoxy-1,4-phenylene)di-(1E)-2,1-ethenediyl]bis-
- CAS Number:1202253-60-8
- Molecular formula:C26H22O6
- Molecular Weight:430.46
![Benzoic acid, 4,4'-[(2,5-dimethoxy-1,4-phenylene)di-(1E)-2,1-ethenediyl]bis-, 1,1'-dimethyl ester](/CAS/20240320/GIF/1219033-72-3.gif)
1219033-72-3
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1202253-60-8
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Yield:1202253-60-8 83%
Reaction Conditions:
Stage #1: dimethyl 4,4'-(1E,1'E)-2,2'-(2,5-dimethoxy-1,4-phenylene)bis(ethane-2,1-diyl)dibenzoatewith water;potassium hydroxide in tetrahydrofuran;methanol;Reflux;
Stage #2: with hydrogenchloride in water;
References:
White, Kiley A.;Chengelis, Demetra A.;Zeller, Matthias;Geib, Steven J.;Szakos, Jessica;Petoud, Stephane;Rosi, Nathaniel L. [Chemical Communications,2009,# 30,p. 4506 - 4508] Location in patent:supporting information; experimental part
1075-49-6
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$17.00/1g
51560-21-5
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$55.00/1g
1202253-60-8
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