(R)-(4-chloro-2-fluorophenyl)(cyclopropyl)methanamine synthesis

1synthesis methods

Product Name:(R)-(4-chloro-2-fluorophenyl)(cyclopropyl)methanamine
CAS Number:1213360-40-7
Molecular formula:C10H11ClFN
Molecular Weight:199.65

61072-56-8 Synthesis

61072-56-8
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(R)-(4-chloro-2-fluorophenyl)(cyclopropyl)methanamine

1213360-40-7
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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: titanium(IV) tetraethanolate / dichloromethane
1.2: 0.5 h
2.1: tetrahydrofuran / 6.5 h / -75 - 20 °C
3.1: hydrogenchloride / ethyl acetate

References:

WO2013/64543,2013,A1

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