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ChemicalBook CAS DataBase List ETHYL 3-FORMYL-6-METHYL-4-PHENYL-2-THIOXO-1,2,3,4-TETRAHYDRO-5-PYRIMIDINECARBOXYLATE
123044-10-0

ETHYL 3-FORMYL-6-METHYL-4-PHENYL-2-THIOXO-1,2,3,4-TETRAHYDRO-5-PYRIMIDINECARBOXYLATE synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: hydrogenchloride; aluminum (III) chloride / methanol; water / 4 h / Reflux
2: trichlorophosphate / 0.67 h / 70 °C / Cooling with ice

References:

Satyavathi;Naga Ravi Kiran;Bhoja Raju;Sharmila [Asian Journal of Chemistry,2010,vol. 22,# 7,p. 5182 - 5186]