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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List MethanesulfonaMide, N-[5-[4-[5-[[(2R,6S)-2,6-diMethyl-4-Morpholinyl]Methyl]-2-oxazolyl]-1H-indazol-6-yl]-2-Methoxy-3-pyridinyl]-, rel-
1254036-66-2

MethanesulfonaMide, N-[5-[4-[5-[[(2R,6S)-2,6-diMethyl-4-Morpholinyl]Methyl]-2-oxazolyl]-1H-indazol-6-yl]-2-Methoxy-3-pyridinyl]-, rel- synthesis

12synthesis methods
884495-39-0 Synthesis
5-BROMO-2-METHOXY-3-CYANOPYRIDINE

884495-39-0
170 suppliers
$5.00/1g

MethanesulfonaMide, N-[5-[4-[5-[[(2R,6S)-2,6-diMethyl-4-Morpholinyl]Methyl]-2-oxazolyl]-1H-indazol-6-yl]-2-Methoxy-3-pyridinyl]-, rel-

1254036-66-2
49 suppliers
$35.00/1mg

-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / 1,4-dioxane / 2 h / 80 °C / Inert atmosphere
2.1: pyridine / 18 h / 20 °C
3.1: potassium phosphate; potassium hydrogenfluoride / tricyclohexylphosphine; palladium diacetate / isopropyl alcohol; water / 2 h / 75 - 80 °C / Inert atmosphere
4.1: sodium hydroxide; water / 3.08 h / 17 - 23 °C
4.2: 30 °C / pH 6.6

References:

GLAXO GROUP LIMITED;HAMBLIN, Julie Nicole;JONES, Paul Spencer;KEELING, Suzanne Elaine;LE, Joelle;MITCHELL, Charlotte Jane;PARR, Nigel James;WILLACY, Robert David WO2012/32067, 2012, A1

5-Oxazolemethanol, 2-[6-chloro-1-(phenylsulfonyl)-1H-indazol-4-yl]-

1254036-83-3
2 suppliers
inquiry

MethanesulfonaMide, N-[5-[4-[5-[[(2R,6S)-2,6-diMethyl-4-Morpholinyl]Methyl]-2-oxazolyl]-1H-indazol-6-yl]-2-Methoxy-3-pyridinyl]-, rel-

1254036-66-2
49 suppliers
$35.00/1mg

References
4-[5-(bromomethyl)-2-oxazolyl]-6-chloro-1-(phenylsulfonyl)-1H-Indazole

1254036-84-4
2 suppliers
inquiry

MethanesulfonaMide, N-[5-[4-[5-[[(2R,6S)-2,6-diMethyl-4-Morpholinyl]Methyl]-2-oxazolyl]-1H-indazol-6-yl]-2-Methoxy-3-pyridinyl]-, rel-

1254036-66-2
49 suppliers
$35.00/1mg

References
6-Chloro-4-iodo-1H-indazole

885519-56-2
110 suppliers
$18.00/250mg

MethanesulfonaMide, N-[5-[4-[5-[[(2R,6S)-2,6-diMethyl-4-Morpholinyl]Methyl]-2-oxazolyl]-1H-indazol-6-yl]-2-Methoxy-3-pyridinyl]-, rel-

1254036-66-2
49 suppliers
$35.00/1mg

References
6-chloro-4-iodo-1-(phenylsulfonyl)-1H-Indazole

1254036-94-6
2 suppliers
inquiry

MethanesulfonaMide, N-[5-[4-[5-[[(2R,6S)-2,6-diMethyl-4-Morpholinyl]Methyl]-2-oxazolyl]-1H-indazol-6-yl]-2-Methoxy-3-pyridinyl]-, rel-

1254036-66-2
49 suppliers
$35.00/1mg

References