ChemicalBook CAS DataBase List 2-(2-Chloro-3,5-diMethylphenyl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane

2-(2-Chloro-3,5-diMethylphenyl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane synthesis

1synthesis methods

Product Name:2-(2-Chloro-3,5-diMethylphenyl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane
CAS Number:1256781-74-4
Molecular formula:C14H20BClO2
Molecular Weight:266.57

2-(3,5-DIMETHYLPHENYL)-4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLANE

325142-93-6
46 suppliers
$45.00/100mg

2-(2-Chloro-3,5-diMethylphenyl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane

1256781-74-4
44 suppliers
$140.00/100mg

Yield:1256781-74-4 64%

Reaction Conditions:

with gold(III) chloride;N-chloro-succinimide in 1,2-dichloro-ethane at 80; for 48 h;regioselective reaction;

References:

Qiu, Di;Mo, Fanyang;Zheng, Zhitong;Zhang, Yan;Wang, Jianbo [Organic Letters,2010,vol. 12,# 23,p. 5474 - 5477] Location in patent:supporting information; experimental part