ChemicalBook CAS DataBase List 1-Bromo-4,4,5,5,6,6,6-heptafluoro-3,3-bis(trifluoromethyl)hex-1-ene

1-Bromo-4,4,5,5,6,6,6-heptafluoro-3,3-bis(trifluoromethyl)hex-1-ene synthesis

1synthesis methods

Product Name:1-Bromo-4,4,5,5,6,6,6-heptafluoro-3,3-bis(trifluoromethyl)hex-1-ene
CAS Number:128454-94-4
Molecular formula:C8H2BrF13
Molecular Weight:424.98

2-BROMO-1,1,1,3,3,4,4,5,5,5-DECAFLUORO-2-(TRIFLUOROMETHYL)PENTANE

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1-Bromo-4,4,5,5,6,6,6-heptafluoro-3,3-bis(trifluoromethyl)hex-1-ene

128454-94-4
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Yield:128454-94-4 90%

Reaction Conditions:

with tetrabutylammomium bromide in dichloromethane at 80; for 7 h;other nucleophiles possible (NaN₃, NaNO₂, KSCN, KCN), other solvents possible (C₂H₄Cl₂, ethyl acetate);

References:

Rozhkov, I. N.;Igumnov, S. M.;Pletnev, S. I.;Chaplina, I. V. [Bulletin of the Academy of Sciences of the USSR Division of Chemical Science,1990,vol. 39,# 4.2,p. 856][Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya,1990,# 4,p. 951]

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