2,3,4,6-Tetra-O-benzyl-5-thio-D-glucono-1,5-lactone synthesis
- Product Name:2,3,4,6-Tetra-O-benzyl-5-thio-D-glucono-1,5-lactone
- CAS Number:131757-92-1
- Molecular formula:C34H34O5S
- Molecular Weight:554.7
102029-58-3
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Yield:-
Steps:
Multi-step reaction with 6 steps
1: 66 percent / 0.05M NaOMe / methanol / 9 h / Ambient temperature
2: 1.) thiourea, 2.) KOAc / 1.) MeOH, RT, 5d, 2.) AcOH, 140 deg C, 19h
3: 31 percent / 2.8percent HCl / H2O / 5 h / Heating
4: 1.) NaH / 1.) DMF, 2.) RT
5: 50 percent / 1M H2SO4 / acetic acid / 4 h / 90 °C
6: 77 percent / DMSO/acetic anhydride / 42 h / Ambient temperature
References:
Yuasa, Hideya;Tamura, Jun-ichi;Hashimoto, Hironobu [Journal of the Chemical Society. Perkin transactions I,1990,# 10,p. 2763 - 2769]
10227-18-6
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131757-92-1
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10227-17-5
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$45.00/250mg
131757-92-1
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16713-80-7
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$55.00/5 g
131757-92-1
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131757-84-1
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131757-92-1
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