2-BroMo-2-(6-chlorophenyl-2,3,4,5-d4)-cyclohexanone synthesis
- Product Name:2-BroMo-2-(6-chlorophenyl-2,3,4,5-d4)-cyclohexanone
- CAS Number:1336986-08-3
- Molecular formula:C12H8BrClD4O
- Molecular Weight:291.6047
1219795-51-3
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1336986-08-3
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Yield:-
Steps:
Multi-step reaction with 5 steps
1.1: iodine; magnesium / tetrahydrofuran / 0.5 h / 10 - 15 °C
1.2: 16 h / 0 - 25 °C
2.1: toluene-4-sulfonic acid / benzene / 3 h / Reflux
3.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 25 °C
4.1: water; hydrogen bromide / chloroform / 0.5 h / 20 °C
5.1: pyridinium chlorochromate / dichloromethane / 13 h / 20 °C
References:
Sulake, Rohidas S.;Chen, Chinpiao;Lin, Huei-Ru;Lua, Ahai-Chang [Bioorganic and Medicinal Chemistry Letters,2011,vol. 21,# 19,p. 5719 - 5721]
1336986-05-0
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1336986-08-3
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1336986-06-1
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1336986-08-3
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![1-(6-Chlorophenyl-2,3,4,5-d4)-7-oxabicyclo[4.1.0]heptane](/CAS/GIF/1336986-07-2.gif)
1336986-07-2
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1336986-08-3
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108-94-1
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$12.00/50g
1336986-08-3
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