3-Ethyl 2-Methyl 6-hydroxy-3,4-dihydroisoquinoline-2,3(1H)-dicarboxylate synthesis

3synthesis methods

Product Name:3-Ethyl 2-Methyl 6-hydroxy-3,4-dihydroisoquinoline-2,3(1H)-dicarboxylate
CAS Number:134388-88-8
Molecular formula:C14H17NO5
Molecular Weight:279.29

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 70 percent / 0.05 N HCl / 0.75 h / Heating
2: 237.3 g / HCl / Heating
3: i-Pr₂NEt / CH₂Cl₂ / 0.33 h / 0 °C

References:

Ornstein;Arnold;Augenstein;Paschal [Journal of Organic Chemistry,1991,vol. 56,# 14,p. 4388 - 4392]

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