Methyl 3-(6-methyl-4,8-dioxo-1,3,6,2-dioxazaborocan-2-yl) benzoate synthesis
2synthesis methods
- Product Name:Methyl 3-(6-methyl-4,8-dioxo-1,3,6,2-dioxazaborocan-2-yl) benzoate
- CAS Number:1356823-24-9
- Molecular formula:C13H14BNO6
- Molecular Weight:291.0644
Yield:99-36-5 83%
Reaction Conditions:
with C21H30ClNPPd;potassium tert-butylate in tert-Amyl alcohol at 65; for 18 h;Sealed tube;Inert atmosphere;Glovebox;
References:
Haydl, Alexander M.;Hartwig, John F. [Organic Letters,2019,vol. 21,# 5,p. 1337 - 1341] Location in patent:supporting information
![Benzoic acid, 3-benzo[b]thien-3-yl-, methyl ester](/CAS/20210305/GIF/24251-07-8.gif)