ChemicalBook CAS DataBase List 4-[2-methoxy-5-nitro-4-(1-aminoethyl)phenoxy]butanoic acid methyl ester hydrochloride

4-[2-methoxy-5-nitro-4-(1-aminoethyl)phenoxy]butanoic acid methyl ester hydrochloride synthesis

1synthesis methods

Product Name:4-[2-methoxy-5-nitro-4-(1-aminoethyl)phenoxy]butanoic acid methyl ester hydrochloride
CAS Number:1383543-83-6
Molecular formula:C14H21ClN2O6
Molecular Weight:348.78

Butanoic acid, 4-[2-methoxy-5-nitro-4-[1-[(2,2,2-trifluoroacetyl)amino]ethyl]phenoxy]-, methyl ester

162827-96-5
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4-[2-methoxy-5-nitro-4-(1-aminoethyl)phenoxy]butanoic acid methyl ester hydrochloride

1383543-83-6
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Yield:1383543-83-6 97%

Reaction Conditions:

with hydrogenchloride in methanol; for 36 h;Inert atmosphere;Reflux;Solvolysis;

References:

Golkowski, Martin;Pergola, Carlo;Werz, Oliver;Ziegler, Thomas [Organic and Biomolecular Chemistry,2012,vol. 10,# 23,p. 4496 - 4499] Location in patent:supporting information; experimental part

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