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1390657-38-1

3-Pyridinecarboxylic acid, 4,6-dichloro-2-formyl-, ethyl ester synthesis

3synthesis methods
686279-09-4 Synthesis
4,6-DICHLORO-2-METHYL-NICOTINIC ACID ETHYL ESTER

686279-09-4
107 suppliers
$50.00/250mg

3-Pyridinecarboxylic acid, 4,6-dichloro-2-formyl-, ethyl ester

1390657-38-1
10 suppliers
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 24 h / 85 °C
2: N-methylpiperidine-N-oxide / acetonitrile / 1 h / 20 °C / Molecular sieve

References:

ABBOTT LABORATORIES;ABBOTT LABORATORIES TRADING (SHANGHAI) COMPANY, LTD.;VASUDEVAN, Anil;PENNING, Thomas Dale;CHEN, Huanming;LIANG, Bo;WANG, Shaohui;ZHAO, Zhongqiang;CHAI, Dikun;YANG, Leifu;GAO, Yingxiang WO2012/97682, 2012, A1

1390657-37-0 Synthesis
3-Pyridinecarboxylic acid, 2-(bromomethyl)-4,6-dichloro-, ethyl ester

1390657-37-0
4 suppliers
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3-Pyridinecarboxylic acid, 4,6-dichloro-2-formyl-, ethyl ester

1390657-38-1
10 suppliers
inquiry