ChemicalBook CAS DataBase List 4(1H)-QUINAZOLINONE, 3-(2-(4-(4-NITROBENZOYL)-1-PIPERIDINYL)ETHYL)-2,3-DIHYDRO-2-THIOXO-

4(1H)-QUINAZOLINONE, 3-(2-(4-(4-NITROBENZOYL)-1-PIPERIDINYL)ETHYL)-2,3-DIHYDRO-2-THIOXO- synthesis

3synthesis methods

Product Name:4(1H)-QUINAZOLINONE, 3-(2-(4-(4-NITROBENZOYL)-1-PIPERIDINYL)ETHYL)-2,3-DIHYDRO-2-THIOXO-
CAS Number:139418-53-4
Molecular formula:C22H22N4O4S
Molecular Weight:438.5

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4(1H)-QUINAZOLINONE, 3-(2-(4-(4-NITROBENZOYL)-1-PIPERIDINYL)ETHYL)-2,3-DIHYDRO-2-THIOXO-

139418-53-4
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Yield:-

Steps:

Multi-step reaction with 5 steps
1: 61 percent / mol. sieves / (Allyl-PdCl)2 / tetrahydrofuran
2: 84 percent / HCl / ethanol
3: 85 percent / K₂CO₃ / dimethylformamide
4: HBr
5: tetrahydrofuran

References:

Huang;Mathis [Journal of labelled compounds and radiopharmaceuticals,1999,vol. 42,# SUPPL. 1,p. S406-S408]

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139418-53-4
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References

Methanone, (1-benzoyl-4-piperidinyl)(4-nitrophenyl)-

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139418-53-4
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References

4(1H)-QUINAZOLINONE, 3-(2-(4-(4-NITROBENZOYL)-1-PIPERIDINYL)ETHYL)-2,3-DIHYDRO-2-THIOXO- Related Search:

1-(2-PIPERIDINOETHYL)-2-THIOUREA

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