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.alpha.-D-Glucopyranoside, phenyl 1-thio-, tetraacetate synthesis

6synthesis methods
-

Yield:13992-16-0 70%

Reaction Conditions:

with potassium phosphate;1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)-2-trisilanol;(2r,4s,5r)-2,4,5,6-Tetrakis(3,6-dichloro-9H-carbazol-9-yl)isophthalonitrile in water;1,2-dichloro-ethane at -5; for 24 h;Inert atmosphere;Irradiation;stereoselective reaction;

References:

Bi, Fangchao;Gao, Feng;Ji, Peng;Wang, Wei;Zhang, Yueteng [Chemical Science,2020,vol. 11,# 48,p. 13079 - 13084]