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ChemicalBook CAS DataBase List (4S,6R)-6-HydroxyMethyl-2,2-diMethyl-1,3-dioxane-4-acetic Acid, 1,1-DiMethylethyl Ester
148809-28-3

(4S,6R)-6-HydroxyMethyl-2,2-diMethyl-1,3-dioxane-4-acetic Acid, 1,1-DiMethylethyl Ester synthesis

1synthesis methods
-

Yield:148809-28-3 95%

Reaction Conditions:

with pyridine;pyridine hydrogenfluoride in tetrahydrofuran at 0; for 4 h;Inert atmosphere;

References:

Szpilman, Alex M.;Cereghetti, Damiano M.;Manthorpe, Jeffrey M.;Wurtz, Nicholas R.;Carreira, Erick M. [Chemistry - A European Journal,2009,vol. 15,# 29,p. 7117 - 7128] Location in patent:supporting information; experimental part