1,3-Dioxolo4,5-cpyridine-4-methanol, hexahydro-7-hydroxy-2,2-dimethyl-, 3aS-(3a.alpha.,4.beta.,7.alpha.,7a.alpha.)- synthesis

Yield:151252-19-6 76%

Reaction Conditions:

with 1% Pd/C;hydrogen;benzylamine in methanol at 20; under 760.051 Torr; for 72 h;

References:

Schitter, Georg;Scheucher, Elisabeth;Steiner, Andreas J.;Stuetz, Arnold E.;Thonhofer, Martin;Wrodnigg, Tanja M.;Tarling, Chris A.;Withers, Stephen G.;Wicki, Jacqueline;Fantur, Katrin;Paschke, Eduard;Mahuran, Don J.;Rigat, Brigitte A.;Tropak, Michael [Beilstein Journal of Organic Chemistry,2010,vol. 6,art. no. 21] Location in patent:supporting information; experimental part