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15340-83-7

Phenanthrene, 1,2,3,4,4a,9,10,10a-octahydro-7-methoxy-1,1,4a-trimethyl-8-(1-methylethyl)-, (4aS,10aS)- synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: (i) SOCl2, Et2O, (ii) /BRN= 610776/, benzene
2: (i) nBuLi, hexane, (ii) /BRN= 2500450/, benzene
3: H2 / Pd-C / ethanol
4: AlCl3 / CH2Cl2

References:

Matsumoto,T.;Suetsugu,A. [Bulletin of the Chemical Society of Japan,1979,vol. 52,p. 1450 - 1453]