ChemicalBook CAS DataBase List 3S-(3a,3a,6a)]-Hexahydrofuro[2,3-b]furan-3-ol Acetate

3S-(3a,3a,6a)]-Hexahydrofuro[2,3-b]furan-3-ol Acetate synthesis

2synthesis methods

Product Name:3S-(3a,3a,6a)]-Hexahydrofuro[2,3-b]furan-3-ol Acetate
CAS Number:162020-29-3
Molecular formula:C8H12O4
Molecular Weight:172.18

109789-17-5 Synthesis

cis-Hexahydro-3-methylene-furo[2,3-b]furan

109789-17-5
12 suppliers
$90.00/10mg

3S-(3a,3a,6a)]-Hexahydrofuro[2,3-b]furan-3-ol Acetate

162020-29-3
10 suppliers
$350.00/25mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) O₃, 2.) Me₂S / 1.) MeOH, CH₂Cl₂, -78 deg C, 1 h, 2.) MeOH, CH₂Cl₂, from -78 deg C to RT
2: NaBH₄ / ethanol / 2 h / 0 °C
3: 45 percent / 1,2-dimethoxy-ethane / 23 °C / immobilized Amano lipase

References:

Ghosh;Kincaid;Walters;Chen;Chaudhuri;Thompson;Culberson;Fitzgerald;Lee;McKee;Munson;Duong;Darke;Zugay;Schleif;Axel;Lin;Huff [Journal of medicinal chemistry,1996,vol. 39,# 17,p. 3278 - 3290]

109789-18-6 Synthesis

FURO[2,3-B]FURAN-3(2H)-ONE, TETRAHYDRO-, CIS-

109789-18-6
1 suppliers
inquiry

162020-29-3
10 suppliers
$350.00/25mg

References

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