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853904-65-1

17-Methyl-5α-androstane-3β,17β-diol-d5 synthesis

3synthesis methods
3β-tert-ButyldiMethylsilyloxy-17-Methyl-5α-androstane-17β-ol-d5

853904-64-0
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17-Methyl-5α-androstane-3β,17β-diol-d5

853904-65-1
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Yield:853904-65-1 86%

Reaction Conditions:

with tetrabutyl ammonium fluoride in tetrahydrofuran at 20; for 20 h;

References:

Felzmann, Wolfgang;Gmeiner, Günter;G?rtner, Peter [Steroids,2005,vol. 70,# 2,p. 103 - 110]