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ChemicalBook CAS DataBase List 1,2,3,4-TETRAHYDRO-NAPHTHALEN-2-YLAMINE HYDROCHLORIDE

1,2,3,4-TETRAHYDRO-NAPHTHALEN-2-YLAMINE HYDROCHLORIDE synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 81 percent / L-Selectride / tetrahydrofuran / 1.) -78 deg C, 4 h, 2.) r.t., 30 min
2: 1.) H2, 2.) H2 / 1.) 10percent Pd/C, 2.) Raney-Ni / 1.) MeOH, r.t., 1 h, 2.) r.t., 4 h, 50 bar

References:

Gmeiner, Peter;Bollinger, Bernd [Liebigs Annalen der Chemie,1992,# 3,p. 273 - 278]

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