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ChemicalBook CAS DataBase List 1-PHENYL-5-(TRIFLUOROMETHYL)PYRAZOLE-4-CARBONYL CHLORIDE

1-PHENYL-5-(TRIFLUOROMETHYL)PYRAZOLE-4-CARBONYL CHLORIDE synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: lithium hydroxide / tetrahydrofuran / 2 h / 70 °C
2: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 20 °C

References:

Tianjian Medical University;Dong, Weili;Cai, Wenxi;Wang, Shuqing;Wang, Runling CN105601618, 2016, A