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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
176966-87-3

(3S,4R)-3-Hydroxy-4-methyl-piperidine-1-carboxylic acid tert-butyl ester synthesis

9synthesis methods
1-Piperidinecarboxylic acid, 3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-4-methyl-, 1,1-dimethylethyl ester, (3S,4R)-

176966-86-2
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(3S,4R)-3-Hydroxy-4-methyl-piperidine-1-carboxylic acid tert-butyl ester

176966-87-3
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Yield:176966-87-3 76%

Reaction Conditions:

with tetrabutyl ammonium fluoride in tetrahydrofuran; for 2 h;Ambient temperature;

References:

Herdeis;Kaschinski;Karla;Lotter [Tetrahedron Asymmetry,1996,vol. 7,# 3,p. 867 - 884]

24211-54-9 Synthesis
(S)-5-HYDROXY-PIPERIDIN-2-ONE

24211-54-9
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(3S,4R)-3-Hydroxy-4-methyl-piperidine-1-carboxylic acid tert-butyl ester

176966-87-3
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References
2-Piperidinone, 5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-, (5S)-

176966-76-0
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(3S,4R)-3-Hydroxy-4-methyl-piperidine-1-carboxylic acid tert-butyl ester

176966-87-3
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References
1(2H)-Pyridinecarboxylic acid, 5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-5,6-dihydro-2-oxo-, 1,1-dimethylethyl ester, (S)- (9CI)

176966-78-2
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(3S,4R)-3-Hydroxy-4-methyl-piperidine-1-carboxylic acid tert-butyl ester

176966-87-3
2 suppliers
inquiry

References
1-Piperidinecarboxylic acid, 5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-2-oxo-, 1,1-dimethylethyl ester, (S)- (9CI)

176966-77-1
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(3S,4R)-3-Hydroxy-4-methyl-piperidine-1-carboxylic acid tert-butyl ester

176966-87-3
2 suppliers
inquiry

References