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188744-91-4

5H-1,3-Dioxolo4,5-cpyrrole-5-carboxylic acid, 4-(3-aminophenyl)-6-(1,1-dimethylethyl)dimethylsilyloxymethyltetrahydro-2,2-dimethyl-, 1,1-dimethylethyl ester, (3aS,4S,6R,6aR)- synthesis

1synthesis methods
5H-1,3-Dioxolo4,5-cpyrrole-5-carboxylic acid, 4-(1,1-dimethylethyl)dimethylsilyloxymethyl-6-3-(di-2-propenylamino)phenyltetrahydro-2,2-dimethyl-, 1,1-dimethylethyl ester, (3aR,4R,6S,6aS)-

188744-89-0
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5H-1,3-Dioxolo4,5-cpyrrole-5-carboxylic acid, 4-(3-aminophenyl)-6-(1,1-dimethylethyl)dimethylsilyloxymethyltetrahydro-2,2-dimethyl-, 1,1-dimethylethyl ester, (3aS,4S,6R,6aR)-

188744-91-4
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inquiry

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Yield:188744-91-4 66%

Reaction Conditions:

with Wilkinson's catalyst in water;acetonitrile; for 4 h;Heating;

References:

Furneaux, Richard H.;Limberg, Gerrit;Tyler, Peter C.;Schramm, Vern L. [Tetrahedron,1997,vol. 53,# 8,p. 2915 - 2930]