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3,5-dibromo-2,2,6,6-tetramethyl-4-piperidone hydrobromide synthesis

1synthesis methods
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Yield: 95%

Reaction Conditions:

Stage #1:2,2,6,6-Tetramethyl-4-piperidone with acetic acid at 20;
Stage #2: with bromine at 20; for 16 h;

References:

Vuong, Wayne;Mosquera-Guagua, Fabricio;Sanichar, Randy;McDonald, Tyler R.;Ernst, Oliver P.;Wang, Lei;Vederas, John C. [Organic Letters,2019,vol. 21,# 24,p. 10149 - 10153] Location in patent:supporting information

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