1H-1,4-Diazepine, 1H-indazole-3-carboxamide deriv. synthesis
- Product Name:1H-1,4-Diazepine, 1H-indazole-3-carboxamide deriv.
- CAS Number:129294-09-3
- Molecular formula:C13H14N5O
- Molecular Weight:256.2832
195132-53-7
7 suppliers
$407.00/1g
129294-09-3
7 suppliers
inquiry
Yield:-
Steps:
Multi-step reaction with 3 steps
1: 93 percent / SOCl2 / CHCl3 / 6 h / Heating
2: 72 percent / ethanol; H2O / 16 h / 50 °C
3: 2.) NaBH4 / 1.) MeOH, RT, 3 h, 2.) MeOH, RT, 18 h
References:
Harada, Hiroshi;Morie, Toshiya;Hirokawa, Yoshimi;Kato, Shiro [Tetrahedron Asymmetry,1997,vol. 8,# 14,p. 2367 - 2374]