1H-BenziMidazole, 2-(3,5-dibroMophenyl)-1-phenyl- synthesis
- Product Name:1H-BenziMidazole, 2-(3,5-dibroMophenyl)-1-phenyl-
- CAS Number:953091-79-7
- Molecular formula:C19H12Br2N2
- Molecular Weight:428.12
Yield:953091-79-7 59.8%
Reaction Conditions:
Stage #1: 3,5-dibromobenzoic acidwith thionyl chloride for 4 h;Reflux;Inert atmosphere;
Stage #2: N-phenyl-1,2-benzenediaminewith triethylamine in tetrahydrofuran at 20; for 24 h;Inert atmosphere;
Stage #3: with acetic acid for 12 h;Reflux;
References:
Tseng, Chih-Yang;Su, Wen-Fen;Chen, Yun [Journal of Polymer Science, Part A: Polymer Chemistry,2017,vol. 55,# 15,p. 2494 - 2505]
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