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137434-61-8

1H-Benzotriazol-4-amine,5-methyl-(9CI) synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 90 percent / conc. H2SO4, 70percent HNO3
2: 68 percent / H2 / 5percent Pd/C / aq. ethanol / 48 h / 3102.9 Torr / Ambient temperature

References:

Katritzky, Alan R.;Ji, Fu-Bao;Fan, Wei-Qiang;Gallos, John K.;Greenhill, John V.;et al. [Journal of Organic Chemistry,1992,vol. 57,# 1,p. 190 - 195]