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1H-Cyclopent[cd]indene synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 60 percent / methanol / 8 h
2: NaH / 1.) MeOH, ether, 2.) 50-60 deg C, 10-3 - 10-4 Torr
3: 600 °C / 0 - 0 Torr

References:

Wentrup, Curt;Benedikt, Jens [Journal of Organic Chemistry,1980,vol. 45,# 8,p. 1407 - 1409]

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