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180681-90-7

1H-Inden-1-ol, 2-bromo-2,3-dihydro-, (1S,2R)- synthesis

10synthesis methods
-

Yield:180681-90-7 93%

Reaction Conditions:

with formic acid;Ms-DENEB;triethylamine in ethyl acetate at 40; for 8 h;Inert atmosphere;stereoselective reaction;

References:

Touge, Taichiro;Nara, Hideki;Kida, Michio;Matsumura, Kazuhiko;Kayaki, Yoshihito [Organic Letters,2021,vol. 23,# 8,p. 3070 - 3075] Location in patent:supporting information