![](/CAS/20180527/GIF/58001-78-8.gif)
(1R,5S)-bicyclo[3.1.0]hexan-2-one synthesis
- Product Name:(1R,5S)-bicyclo[3.1.0]hexan-2-one
- CAS Number:58001-78-8
- Molecular formula:C6H8O
- Molecular Weight:96.13
![(1R,2R,5S)-bicyclo[3.1.0]hexan-2-ol](/CAS/20180527/GIF/741676-78-8.gif)
741676-78-8
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![(1R,5S)-bicyclo[3.1.0]hexan-2-one](/CAS/20180527/GIF/58001-78-8.gif)
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Yield:58001-78-8 95%
Reaction Conditions:
Stage #1: (1R,2R,5S)-bicyclo[3.1.0]hexan-2-olwith dipotassium hydrogenphosphate in tert-butyl methyl ether;water at 0;Large scale;
Stage #2: with sodium hypochlorite;2,2,6,6-Tetramethyl-1-piperidinyloxy free radical in tert-butyl methyl ether;water at 5; pH=10.4;Large scale;
References:
Alorati, Anthony D.;Bio, Matthew M.;Brands, Karel M. J.;Cleator, Ed;Davies, Antony J.;Wilson, Robert D.;Wise, Chris S. [Organic Process Research and Development,2007,vol. 11,# 3,p. 637 - 641]
![4-Oxocyclohexan-1-ol p-toluenesulfonate](/CAS/GIF/23511-04-8.gif)
23511-04-8
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58001-78-8
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![(+)-1,2-epoxyhex-5-ene](/CAS/GIF/137688-20-1.gif)
137688-20-1
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![(1R,5S)-bicyclo[3.1.0]hexan-2-one](/CAS/20180527/GIF/58001-78-8.gif)
58001-78-8
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