(1R,5S)-bicyclo[3.1.0]hexan-2-one synthesis
- Product Name:(1R,5S)-bicyclo[3.1.0]hexan-2-one
- CAS Number:58001-78-8
- Molecular formula:C6H8O
- Molecular Weight:96.13
![(1R,2R,5S)-bicyclo[3.1.0]hexan-2-ol](/CAS/20180527/GIF/741676-78-8.gif)
741676-78-8
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58001-78-8
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Yield:58001-78-8 95%
Reaction Conditions:
Stage #1: (1R,2R,5S)-bicyclo[3.1.0]hexan-2-olwith dipotassium hydrogenphosphate in tert-butyl methyl ether;water at 0;Large scale;
Stage #2: with sodium hypochlorite;2,2,6,6-Tetramethyl-1-piperidinyloxy free radical in tert-butyl methyl ether;water at 5; pH=10.4;Large scale;
References:
Alorati, Anthony D.;Bio, Matthew M.;Brands, Karel M. J.;Cleator, Ed;Davies, Antony J.;Wilson, Robert D.;Wise, Chris S. [Organic Process Research and Development,2007,vol. 11,# 3,p. 637 - 641]
23511-04-8
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58001-78-8
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137688-20-1
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58001-78-8
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![Bicyclo[3.1.0]hexan-2-one, (1S,5R)-](/CAS/20180601/GIF/196488-92-3.gif)