(1S,2S,3S)-2,3-Bis(benzoyloxymethyl)cyclobutanol synthesis
- Product Name:(1S,2S,3S)-2,3-Bis(benzoyloxymethyl)cyclobutanol
- CAS Number:132294-17-8
- Molecular formula:C20H20O5
- Molecular Weight:340.37
132178-71-3
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132294-17-8
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Yield:-
Steps:
Multi-step reaction with 7 steps
1: DCC / CH2Cl2 / Ambient temperature
2: imidazole / dimethylformamide / 1.5 h / 5 °C
3: N2O4, NaOAc / CCl4 / 0.25 h / 5 °C
4: LiBH4 / tetrahydrofuran / Ambient temperature
5: 83 g / pyridine / 2.5 h / Ambient temperature
6: 46.4 g / 0.5 N H2SO4 / acetonitrile / 17 h / Ambient temperature
7: 90 percent / LS-Selectride / tetrahydrofuran / 0.17 h / -78 °C
References:
Bisacchi;Braitman;Cianci;Clark;Field;Hagen;Hockstein;Malley;Mitt;Slusarchyk;Sundeen;Terry;Tuomari;Weaver;Young;Zahler [Journal of Medicinal Chemistry,1991,vol. 34,# 4,p. 1415 - 1421]
132294-16-7
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$95.00/2mg
132294-17-8
11 suppliers
$120.00/2mg
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1013657-42-5
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132294-17-8
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132294-17-8
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132178-73-5
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132294-17-8
11 suppliers
$120.00/2mg