(1S,2S)-FMOC-2-AMINOCYCLOHEXANE CARBOXYLIC ACID synthesis
- Product Name:(1S,2S)-FMOC-2-AMINOCYCLOHEXANE CARBOXYLIC ACID
- CAS Number:312965-07-4
- Molecular formula:C22H23NO4
- Molecular Weight:365.42
![1-Cyclohexene-1-carboxylic acid, 2-[[(1S)-1-phenylethyl]amino]-, ethyl ester](/CAS/20210305/GIF/53898-03-6.gif)
53898-03-6
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312965-07-4
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Yield:-
Steps:
Multi-step reaction with 6 steps
1.1: NaBH4; isobutyric acid / toluene / 3 h / 0 °C
1.2: HBr / ethyl acetate; propionic acid / 0 °C
1.3: aq. NaHCO3
2.1: Na / ethanol / 15 h / 80 °C
3.1: HCl / ethyl acetate; dioxane / 0 - 20 °C
4.1: LiOH*H2O / tetrahydrofuran; ethanol; H2O / 36 h / 0 °C
5.1: HCO2NH4 / Pd/C / methanol / 2 h / Heating
6.1: NaHCO3 / acetone; H2O / 0 - 20 °C
References:
Schinnerl, Marina;Murray, Justin K.;Langenhan, Joseph M.;Gellman, Samuel H. [European Journal of Organic Chemistry,2003,# 4,p. 721 - 726]
1655-07-8
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312965-07-4
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$45.00/5mg
![Cyclohexanecarboxylic acid, 2-[[(1S)-1-phenylethyl]amino]-, ethyl ester, (1S,2S)-](/CAS/20210305/GIF/191986-95-5.gif)
191986-95-5
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312965-07-4
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![Cyclohexanecarboxylic acid, 2-[[(1S)-1-phenylethyl]amino]-, ethyl ester, (1R,2S)-](/CAS/20210305/GIF/191986-93-3.gif)
191986-93-3
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312965-07-4
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$45.00/5mg
488703-61-3
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$45.00/250mg
312965-07-4
55 suppliers
$45.00/5mg