2,2,2-trifluoro-1-(naphthalen-1-yl)ethanol synthesis
- Product Name:2,2,2-trifluoro-1-(naphthalen-1-yl)ethanol
- CAS Number:17556-44-4
- Molecular formula:C12H9F3O
- Molecular Weight:226.19
Yield:17556-44-4 97%
Reaction Conditions:
Stage #1: 1-naphthaldehyde;(trifluoromethyl)trimethylsilanewith tetrabutyl ammonium fluoride in tetrahydrofuran at -20 - 20; for 6 h;
Stage #2: with water in tetrahydrofuran at 0 - 20; for 16 h;
References:
Czerwiński, Pawe?;Molga, Edyta;Cavallo, Luigi;Poater, Albert;Michalak, Micha? [Chemistry - A European Journal,2016,vol. 22,# 24,p. 8089 - 8094] Location in patent:supporting information
185739-16-6
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