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699-35-4

2,2,3,3,4,4-hexafluorocyclobutan-1-one synthesis

2synthesis methods
-

Yield:699-35-4 95.3%

Reaction Conditions:

with sodium hypochlorite at 20; for 1 h;

Steps:

1

The obtained hexafluorocyclobutene was dissolved in a fluorocarbon solvent,Oxidation was carried out using sodium hypochlorite at room temperature for 1 hour.The product was perfluorocyclobutanone (IV) in a yield of 95.3%.

References:

CN105016990,2017,B Location in patent:Paragraph 0024; 0053; 0054; 0055; 0059; 0060; 0061