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2,2-DiMethyl-2H-1,4-benzothiazin-3(4H)-one, 97% synthesis

3synthesis methods
-

Yield:90921-53-2 98%

Reaction Conditions:

with N-methylcyclohexylamine;1,8-diazabicyclo[5.4.0]undec-7-ene at 180; under 7757.22 Torr; for 4 h;microwave irradiation;

References:

Kamila, Sukanta;Koh, Benjamin;Khan, Omair;Zhang, Hongming;Biehl, Edward R. [Journal of Heterocyclic Chemistry,2006,vol. 43,# 6,p. 1641 - 1646]