2,3,4-Tribromo-phenol 1-Acetate synthesis

2synthesis methods

Yield:-

Reaction Conditions:

Stage #1: 3,4-dibromophenolwith bromine;acetic acid at 20; for 1.5 h;
Stage #2: acetic anhydridewith pyridine in dichloromethane at 20; for 2 h;

References:

Liu, Huiling;Bernhardsen, Monica;Fiksdahl, Anne [Tetrahedron,2006,vol. 62,# 15,p. 3564 - 3572]

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