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22109-56-4

2,3,5-Trichloro-6-methylpyridine synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 93 percent / HCl / dimethylformamide / 1 h
2: 89 percent / POCl3 / 4 h / 190 °C

References:

Shvekhgeimer, M.-G. A.;Korbakov, K. I.;Sychev, S. S.;Promonenkov, V. K. [Doklady Chemistry,1987,vol. 294,p. 269 - 273][Dokl. Akad. Nauk SSSR Ser. Khim.,1987,vol. 294,# 4,p. 893 - 897]