2,3-DIHYDRO-1H-INDEN-5-YLACETIC ACID synthesis
- Product Name:2,3-DIHYDRO-1H-INDEN-5-YLACETIC ACID
- CAS Number:5453-98-5
- Molecular formula:C11H12O2
- Molecular Weight:176.21
24425-40-9
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: sodium nitrite; potassium iodide; hydrogenchloride / water / 2 h / 0 - 5 °C
2: manganese; bis(bipyridine)nickel(II) bromide; trifluoroacetic acid / N,N-dimethyl-formamide / 15 h / 50 °C
3: lithium hydroxide / water; tetrahydrofuran / 15 h / 20 °C
References:
Ahn, Songyeon;Kim, Yong Soo;Kim, Myeong Seup;Ann, Jihyae;Ha, Heejin;Yoo, Young Dong;Kim, Young Ho;Blumberg, Peter M.;Frank-Foltyn, Robert;Bahrenberg, Gregor;Stockhausen, Hannelore;Christoph, Thomas;Lee, Jeewoo [Bioorganic and Medicinal Chemistry Letters,2020,vol. 30,# 3,art. no. 126838]
158094-20-3
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858225-07-7
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132464-83-6
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5453-98-5
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