2-[(3-FLUOROBENZYL)OXY]-1H-ISOINDOLE-1,3(2H)-DIONE synthesis
- Product Name:2-[(3-FLUOROBENZYL)OXY]-1H-ISOINDOLE-1,3(2H)-DIONE
- CAS Number:30777-87-8
- Molecular formula:C15H10FNO3
- Molecular Weight:271.24
Yield:30777-87-8 54.8%
Reaction Conditions:
with sodium hydroxide in N,N-dimethyl-formamide;
Steps:
5.2.1.2. Synthetic procedures for compounds 7a-r
General procedure: Compound 7a was synthesized referencing to the literatures [18] and [29]. To be pointed out, the crude products of 7b, 7i, 7k, 7l, 7n-p required to wash with the solution of ethyl acetate/petroleum ether (v/v = 1:5) again;
References:
Wang, Ming-Zhong;Xu, Han;Liu, Tuan-Wei;Feng, Qi;Yu, Shu-Jing;Wang, Su-Hua;Li, Zheng-Ming [European Journal of Medicinal Chemistry,2011,vol. 46,# 5,p. 1463 - 1472] Location in patent:experimental part
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