2,4,6-TRIFLUOROIODOBENZENE synthesis

2synthesis methods

372-38-3 Synthesis

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 89 percent / KI; periodic acid; H₂SO₄ / 4 h / 70 °C
2: various solvent(s) / 16 h / -270.16 °C / Irradiation

References:

Wenk, Hans Henning;Sander, Wolfram [European Journal of Organic Chemistry,2002,# 23,p. 3927 - 3935]

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