2,4,6-TRIS(4-BROMOPHENYL)-1,3,5-TRIAZINE synthesis
- Product Name:2,4,6-TRIS(4-BROMOPHENYL)-1,3,5-TRIAZINE
- CAS Number:30363-03-2
- Molecular formula:C21H12Br3N3
- Molecular Weight:546.05
![1-(tert-butyl)-3-((5-chloro-3-(hydroxymethyl)pyridin-2-yl)methyl)-1,3-dihydro-2H-pyrrolo[2,3-b]pyridin-2-one](/CAS/20180629/GIF/1455358-11-8.gif)
1455358-11-8
15 suppliers
inquiry
30363-03-2
142 suppliers
$8.00/250mg
Yield:30363-03-2 75%
Reaction Conditions:
with bromine;iron;sodium hydroxide in chloroform;Cooling with ice;Darkness;
Steps:
3
Under ice bath and dark conditions,Add to a 500ml three-necked bottle2,4,6-triphenyl-1,3,5-triazine (17.84g, 100mmol),Iron powder (0.83g, 15mmol)And chloroform solvent (500ml),Bring liquid bromine (25.7ml, 500mmol)Add pre-filled 50mlIn the constant pressure funnel of chloroform,Slowly add the mixture dropwise,And use sodium hydroxide solution to treat bromine vapor.After reacting overnight,Add NaHSO3 aqueous solution to stop the reaction,After the system color becomes white,Separate the solids,And washed with methanol,Purify with chlorobenzene,The final product2,4,6-Tris(4-bromophenyl)-1,3,5-triazine(40.9g, yield 75%),
References:
CN113264951,2021,A Location in patent:Paragraph 0023; 0024; 0025
623-00-7
483 suppliers
$6.00/10g
30363-03-2
142 suppliers
$8.00/250mg