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116435-81-5

2-(4-amino-2-nitrophenyl)acetic acid synthesis

5synthesis methods
Imidodicarbonic acid, 2-(4-methyl-3-nitrophenyl)-, 1,3-bis(1,1-dimethylethyl) ester

135685-05-1
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2-(4-amino-2-nitrophenyl)acetic acid

116435-81-5
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 40 percent / N-bromosuccinimide; AIBN / CCl4 / 20 h / Heating
2: 80 percent / triethylammonium sulfate / H2O; CH2Cl2 / 20 °C
3: 70 percent / conc. HCl / 20 h / Heating

References:

Han, Shoufa;Moore, Roger A.;Viola, Ronald E. [Bioorganic Chemistry,2002,vol. 30,# 2,p. 81 - 94]