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ChemicalBook CAS DataBase List 2,4-BIS(BENZYLOXY)PYRIMIDINE

2,4-BIS(BENZYLOXY)PYRIMIDINE synthesis

1synthesis methods
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Yield:7306-79-8 86.6%

Reaction Conditions:

Stage #1: benzyl alcoholwith sodium hydride in tetrahydrofuran;mineral oil at 20; for 0.5 h;
Stage #2: 2,6-Dichloropyrimidine in tetrahydrofuran;mineral oil at 80; for 4 h;

References:

Todorov, Aleksandar R.;Wirtanen, Tom;Helaja, Juho [Journal of Organic Chemistry,2017,vol. 82,# 24,p. 13756 - 13767]

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