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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 2,4-DIMETHYLDIBENZOTHIOPHENE
31317-18-7

2,4-DIMETHYLDIBENZOTHIOPHENE synthesis

10synthesis methods
6320-02-1 Synthesis
2-BROMOTHIOPHENOL

6320-02-1
156 suppliers
$14.00/1g

2,4-DIMETHYLDIBENZOTHIOPHENE

31317-18-7
9 suppliers
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-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: sulfuryl dichloride; triethylamine / dichloromethane / 0 - 20 °C
1.2: 1 h / 0 - 20 °C
2.1: palladium diacetate; trifluoroacetic acid / 0.75 h / 20 °C
3.1: potassium pivalate; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl acetamide / 12 h / 140 °C

References:

Saravanan, Perumal;Anbarasan, Pazhamalai [Organic Letters,2014,vol. 16,# 3,p. 848 - 851]

960203-41-2 Synthesis
1-[(2-Bromophenyl)thio]-2,4-dimethylbenzene

960203-41-2
84 suppliers
$30.00/1g

2,4-DIMETHYLDIBENZOTHIOPHENE

31317-18-7
9 suppliers
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References
Pyrrolidine, 1-[(1E)-2-[3,5-dimethyl-2'-(methylthio)[1,1'-biphenyl]-2-yl]diazenyl]-

1446427-39-9
0 suppliers
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2,4-DIMETHYLDIBENZOTHIOPHENE

31317-18-7
9 suppliers
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References
2,5-Pyrrolidinedione, 1-[(2-bromophenyl)thio]-

1541160-62-6
0 suppliers
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m-Xylene

108-38-3
381 suppliers
$10.60/50gm:

2,4-DIMETHYLDIBENZOTHIOPHENE

31317-18-7
9 suppliers
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References
2-bromocyclohexanone

1056477-06-5
0 suppliers
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2,4-DIMETHYLDIBENZOTHIOPHENE

31317-18-7
9 suppliers
inquiry

References