2,6-dichloro-3-nitrobenzene-1-sulfonyl chloride synthesis

3synthesis methods

Product Name:2,6-dichloro-3-nitrobenzene-1-sulfonyl chloride
CAS Number:276702-53-5
Molecular formula:C6H2Cl3NO4S
Molecular Weight:290.51

6579-54-0 Synthesis

6579-54-0
162 suppliers
$7.00/1g

2,6-dichloro-3-nitrobenzene-1-sulfonyl chloride

276702-53-5
20 suppliers
$53.00/25mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: LiOH / methanol
2.1: H₂SO₄; HNO₃
3.1: KOH
3.2: POCl₃; PCl₅

References:

McCleland, Brent W.;Davis, Roderick S.;Palovich, Michael R.;Widdowson, Katherine L.;Werner, Michelle L.;Burman, Miriam;Foley, James J.;Schmidt, Dulcie B.;Sarau, Henry M.;Rogers, Martin;Salyers, Kevin L.;Gorycki, Peter D.;Roethke, Theresa J.;Stelman, Gary J.;Azzarano, Leonard M.;Ward, Keith W.;Busch-Petersen, Jakob [Bioorganic and Medicinal Chemistry Letters,2007,vol. 17,# 6,p. 1713 - 1717]

2,6-dichloro-3-nitrobenzene-1-sulfonic acid

276702-52-4
7 suppliers
inquiry

276702-53-5
20 suppliers
$53.00/25mg

References

6697-96-7 Synthesis

6697-96-7
14 suppliers
$502.14/5MG

276702-53-5
20 suppliers
$53.00/25mg

References