2,6-Piperazinedione, 1-methyl- synthesis

1synthesis methods

4408-64-4 Synthesis

Yield:62828-00-6 65%

Reaction Conditions:

with formamide under 100 Torr;1.) 120 deg C, 1.25 h, 2.) 150 deg C, 3.75 h;

References:

Houghton, Roy P.;Williams, Emyr [Journal of the Chemical Society. Perkin transactions I,1982,# 11,p. 2693 - 2696]

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