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2-Azidobenzoic acid synthesis

7synthesis methods
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Yield:31162-13-7 100%

Reaction Conditions:

Stage #1: anthranilic acidwith hydrogenchloride;sodium nitrite in water at 0 - 20; for 0.25 h;
Stage #2: with sodium azide in water at 20;

References:

Patel, Bhargav A.;Abel, Biebele;Barbuti, Anna Maria;Velagapudi, Uday Kiran;Chen, Zhe-Sheng;Ambudkar, Suresh V.;Talele, Tanaji T. [Journal of Medicinal Chemistry,2018,vol. 61,# 3,p. 834 - 864]